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  2. New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation

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New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation

    Authors

    • Ahlam Mohammed Yaseen Al-Bayati 1
    • Zuhoor Fathi Al-Taai 2

    1 Department of Chemistry/ College of Science / University of Mosul

    2 Department of Chemistry/ College Education for Pure Science / University of Mosul

,

Document Type : Research Paper

10.33899/berj.2020.167245
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Abstract

New nickel (II) complexes with three mixed ligand {which are 2-Oxime-4 (3- hydroxyl benzlidene) pentane (L2H); 2- chloro benzaldehyde- thiosemicarbazone (T1H) or 3,4- dimethoxy aceto-phenone thiosemicarbazone (T2H); and glycine (GH) or metformin (mf)} have been prepared by applying classical and microwave heating techniques. The resulting compounds have been characterized using analytical, physical and spectral techniques. Complexes of general formulaes [Ni(L2H)(TH)(BH)](Ac)2 in slightly neutral medium and complexes of general formula [Ni(L2)(T)(mf)] and [Ni(L2)(TH)(G)] in basic medium have been resulted. {where BH= GH or mf ligand, TH= T1H or T2H ligand, L2= deprotonated L2H ligand, T= deprotonated T1H or T2H ligand, G= deprotonated GH ligand}, high spin octahedral complexes have been resulted. No laser He-Ne type (wave length are 600- 700 nm) have been observed on the compounds, this means that the compounds are stable. Biological activity of the ligands and complexes have been evaluated using agar plate diffusion technique against Echerichia coli, Klipsila pnnemoia, Staphylococcus aureus and Pseudomonas aeruginosa. Some compounds were found to have antibacterial activity.

Keywords

  • Ni(II) complexes
  • mixed ligand
  • 2-Oxime-4 (3- hydroxyl benzlidene) pentane

Main Subjects

  • Inorganic chemistry
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College Of  Basic  Education  Research Journal
Volume 16, Issue 4
November 2020
Page 949-964
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APA

Al-Bayati, A., & Al-Taai, Z. (2020). New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation. College Of Basic Education Research Journal, 16(4), 949-964. doi: 10.33899/berj.2020.167245

MLA

Ahlam Mohammed Yaseen Al-Bayati; Zuhoor Fathi Al-Taai. "New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation". College Of Basic Education Research Journal, 16, 4, 2020, 949-964. doi: 10.33899/berj.2020.167245

HARVARD

Al-Bayati, A., Al-Taai, Z. (2020). 'New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation', College Of Basic Education Research Journal, 16(4), pp. 949-964. doi: 10.33899/berj.2020.167245

VANCOUVER

Al-Bayati, A., Al-Taai, Z. New Complexes of Nickel (II) with Mixed Ligands(2-oxime-4-(hydroxl benzilidine)pentane and (Thiosemicarbazones) and (Glycine) or(Metformine),Evaluation of Biological Activites and laser Irradiation. College Of Basic Education Research Journal, 2020; 16(4): 949-964. doi: 10.33899/berj.2020.167245

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